N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

Base Information

Chemical Name:N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine
CAS No.:127559-15-3
Molecular Formula:C₃₁H₂₉NO₇
Molecular Weight:527.574
Hs Code.:

Synonyms:N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

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Chemical Property of N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

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Technology Process of N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

There total 8 articles about N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 120385-11-7
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine methyl ester

: 127559-15-3
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(01)93447-1

Reference yield:

: 1005-30-7
sodium 4-iodo-benzoate

: 127559-15-3
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / CuBr*Me₂S / nitrobenzene / 8 h / 130 °C

2: 89 percent / BH₃*THF / tetrahydrofuran / 3 h / 0 °C

3: 92 percent / LiOH, H₂O / tetrahydrofuran; methanol

With lithium hydroxide; borane-THF; copper(I) bromide dimethylsulfide complex; water; In tetrahydrofuran; methanol; nitrobenzene;
DOI:10.1016/S0040-4039(01)93447-1

Reference yield:

: 105229-41-2
2-Benzyloxycarbonylamino-3-(4-benzyloxy-3-hydroxy-phenyl)-propionic acid methyl ester

: 127559-15-3
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-(hydroxymethyl)phenoxy>-L-tyrosine

Guidance literature:: Multi-step reaction with 3 steps

2: 89 percent / BH₃*THF / tetrahydrofuran / 1) 1 h, 0 deg C 2) to 25 deg C, 2 h

3: 92 percent / LiOH*H₂O / tetrahydrofuran; methanol; H₂O / 0.5 h / 25 °C

With lithium hydroxide; borane-THF; In tetrahydrofuran; methanol; water;
DOI:10.1021/jo00311a019