2-Methylbenzamidine hydrochloride

Base Information

• Chemical Name: 2-Methylbenzamidine hydrochloride
• CAS No.: 18636-98-1
• Molecular Formula: C8H10N2^.HCl
• Molecular Weight: 170.642
• Hs Code.: 2925290090
• Mol file: 18636-98-1.mol

Synonyms:Benzenecarboximidamide,2-methyl-, monohydrochloride (9CI);o-Toluamidine, monohydrochloride (8CI);2-Methylbenzamidine hydrochloride;

Chemical Property of 2-Methylbenzamidine hydrochloride

Chemical Property:

• Vapor Pressure: 0.00555mmHg at 25°C
• Boiling Point: 269.7 °C at 760 mmHg
• Flash Point: 116.9 °C
• PSA: 49.87000
• LogP: 2.88110
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-methylbenzamidinehydrochloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methylbenzamidine hydrochloride

There total 1 articles about 2-Methylbenzamidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-methylbenzamidine (18636-97-0) → 2-methylbenzimidamide hydrochloride (18636-98-1)

Guidance literature:

With hydrogenchloride; In diethyl ether; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201410607

Reference yield: 96.0%

3,3,3-trifluoro-1-(4-methylphenyl)propan-1-one (121194-34-1) + 2-methylbenzimidamide hydrochloride (18636-98-1) → 4-fluoro-2-(o-tolyl)-6-(p-tolyl)pyrimidine

Guidance literature:

With potassium hydrogencarbonate; In 1,4-dioxane; at 60 ℃; for 24h;

DOI:10.1055/s-0039-1690248

Reference yield: 91.0%

2-methylquinoline (91-63-4) + 2-methylbenzimidamide hydrochloride (18636-98-1) → 5-(quinolin-2-yl)-3-(o-tolyl)-1,2,4-thiadiazole

Guidance literature:

With potassium phosphate tribasic trihydrate; sulfur; In dimethyl sulfoxide; for 12h; Heating;

DOI:10.1021/acs.orglett.6b00806

upstream raw materials:

2-methylbenzamidine

Downstream raw materials:

2-(4-methylphenyl)-quinazoline

2-(4-nitrophenyl)-4-(o-tolyl)-1,3,5-triazine

2,4-di-(o-tolyl)-1,3,5-triazine

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