3-acetamido-4-nitrophthalic anhydride

Base Information

Chemical Name:3-acetamido-4-nitrophthalic anhydride
CAS No.:209324-66-3
Molecular Formula:C₁₀H₆N₂O₆
Molecular Weight:250.167
Hs Code.:

Synonyms:3-acetamido-4-nitrophthalic anhydride

Suppliers and Price of 3-acetamido-4-nitrophthalic anhydride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-(5-Nitro-1,3-dioxo-1,3-dihydroisobenzofuran-4-yl)acetamide 97%
1g
$ 680.00

Crysdot
N-(5-Nitro-1,3-dioxo-1,3-dihydroisobenzofuran-4-yl)acetamide 97%
250mg
$ 272.00

Adipogen Life Sciences
3-Acetamido-4-nitrophthalicanhydride ≥98%(HPLC)
1 g
$ 941.00

Total 2 raw suppliers

Chemical Property of 3-acetamido-4-nitrophthalic anhydride

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

N-(5-Nitro-1,3-dioxo-1,3-dihydroisobenzofuran-4-yl)acetamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-acetamido-4-nitrophthalic anhydride

There total 4 articles about 3-acetamido-4-nitrophthalic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 75-36-5
acetyl chloride

: 209324-65-2
3-acetamido-4-nitrophthalic acid

: 209324-66-3
3-acetamido-4-nitrophthalic anhydride

Guidance literature:: In dichloromethane; acetic anhydride;

Reference yield: 56.0%

: 209324-65-2
3-acetamido-4-nitrophthalic acid

: 209324-66-3
3-acetamido-4-nitrophthalic anhydride

Guidance literature:: With acetic anhydride; acetyl chloride; at 80 ℃; for 2h;
DOI:10.1021/ac9801723

Reference yield:

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 209324-66-3
3-acetamido-4-nitrophthalic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / acetic acid / 1 h / Heating

2: 52 percent / KMnO₄; MgSO₄ / H₂O / Heating

3: 56 percent / Ac₂O; AcCl / 2 h / 80 °C

With potassium permanganate; acetic anhydride; magnesium sulfate; acetyl chloride; In water; acetic acid; 1: Substitution / 2: Oxidation / 3: Cyclization;
DOI:10.1021/ac9801723