4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

Base Information

Chemical Name:4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate
CAS No.:10176-68-8
Molecular Formula:C₂₆H₂₄O₉
Molecular Weight:480.471
Hs Code.:

Synonyms:4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

There total 6 articles about 4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6962-57-8
3,6-dihydroxy-2,4-dimethoxyacetophenone

: 100-07-2
4-methoxy-benzoyl chloride

: 10176-68-8
4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

Guidance literature:: 3,6-dihydroxy-2,4-dimethoxyacetophenone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - -10 ℃; for 3h;

4-methoxy-benzoyl chloride; In tetrahydrofuran; at -78 - 20 ℃;

Reference yield:

: 530-55-2,26547-64-8
2,6-dimethoxy-p-quinone

: 10176-68-8
4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc; hydrogenchloride / 0.08 h

2.1: boron trifluoride diethyl etherate / 3 h / 120 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 - -10 °C

3.2: -78 - 20 °C

With hydrogenchloride; boron trifluoride diethyl etherate; lithium hexamethyldisilazane; zinc; In tetrahydrofuran;

Reference yield:

: 7702-17-2
4-(acetyloxy)-3,5-dimethoxyphenyl acetate

: 100-07-2
4-methoxy-benzoyl chloride

: 10176-68-8
4-hydroxy-2,6-dimethoxy-3-(3-(4-methoxyphenyl)-3-oxopropanoyl)phenyl 4-methoxybenzoate

Guidance literature:: 4-(acetyloxy)-3,5-dimethoxyphenyl acetate; With boron trifluoride diethyl etherate; In toluene; at 110 ℃; for 18h;

With water; In toluene; Inert atmosphere;

4-methoxy-benzoyl chloride; Further stages;
DOI:10.1021/op4003642