(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

Base Information

Chemical Name:(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide
CAS No.:1401094-71-0
Molecular Formula:C₂₁H₂₄F₃N₂O₃PS
Molecular Weight:472.468
Hs Code.:

Synonyms:(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

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Chemical Property of (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

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Technology Process of (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

There total 7 articles about (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 421-85-2
Trifluoromethanesulfonamide

: 1401094-73-2
3-{(2S)-2-[(diphenylphosphino)methyl]pyrrolidin-1-yl}propanoic acid

: 1401094-71-0
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 60261-46-3
(2S)-2-[(diphenylphosphino)methyl]pyrrolidine

: 1401094-71-0
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 30 °C

2: sodium hydroxide; methanol / 20 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate / dichloromethane / 0 - 20 °C

With methanol; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In dichloromethane;

Reference yield:

: 1401094-72-1
methyl 3-{(2S)-2-[(diphenylphosphino)methyl]pyrrolidin-1-yl}-propanoate

: 1401094-71-0
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; methanol / 20 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate / dichloromethane / 0 - 20 °C

With methanol; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In dichloromethane;