(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

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Chemical Name:(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide
CAS No.:1401094-60-7
Molecular Formula:C₂₃H₂₄AuF₉N₃O₇PS₃
Molecular Weight:949.583
Hs Code.:

Synonyms:(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

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Chemical Property of (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

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Technology Process of (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

There total 8 articles about (3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1438408-57-1
C₂₁H₂₄AuClF₃N₂O₃PS

: 82113-65-3
bis(trifluoromethanesulfonyl)amide

: 1401094-60-7
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

Guidance literature:: bis(trifluoromethanesulfonyl)amide; With silver (II) carbonate; In dichloromethane; for 0.0833333h; Inert atmosphere; Darkness;

C₂₁H₂₄AuClF₃N₂O₃PS; In dichloromethane; for 2h; Inert atmosphere; Darkness;
DOI:10.1039/c3ob27460h

Reference yield:

: 1401094-73-2
3-{(2S)-2-[(diphenylphosphino)methyl]pyrrolidin-1-yl}propanoic acid

: 1401094-60-7
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18.25 h / 0 - 20 °C / Inert atmosphere

2.1: dichloromethane / 3 h / Inert atmosphere

3.1: silver (II) carbonate / dichloromethane / 0.08 h / Inert atmosphere; Darkness

3.2: 2 h / Inert atmosphere; Darkness

With silver (II) carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1039/c3ob27460h

Reference yield:

: 1401094-71-0
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide

: 1401094-60-7
(3-((2S)-2-((diphenylphosphino)methyl)pyrrolidin-1-ium-1-yl)-propanoyl)((trifluoromethyl)sulfonyl)amide gold bis-triflic amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 3 h / Inert atmosphere

2.1: silver (II) carbonate / dichloromethane / 0.08 h / Inert atmosphere; Darkness

2.2: 2 h / Inert atmosphere; Darkness

With silver (II) carbonate; In dichloromethane;
DOI:10.1039/c3ob27460h