Technology Process of C19H30N2O4
There total 1 articles about C19H30N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(2-benzyloxycarbonylamino-1,1-dimethyl-ethyl)-carbamic acid tert-butyl ester; methyl iodide;
With
sodium hydride;
In
N,N-dimethyl-formamide;
for 2h;
Cooling with ice;
With
water; ammonium chloride;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / palladium on activated charcoal / methanol / 3 h
2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C
With
hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium on activated charcoal / methanol / 3 h
2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C
3.1: trifluoroacetic acid / chloroform / 2 h / 0 °C / Cooling with ice
3.2: 3 h / 50 °C
With
hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; chloroform; N,N-dimethyl-formamide;