N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide

Base Information

• Chemical Name: N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide
• CAS No.: 1607483-32-8
• Molecular Formula: C₁₄H₁₁BrN₂O₃
• Molecular Weight: 335.157
• Mol file: 1607483-32-8.mol

Synonyms:N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide

Chemical Property of N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide

Chemical Property:

Purity/Quality:

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Technology Process of N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide

There total 1 articles about N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-hydroxy-3-bromobenzaldehyde (1829-34-1) + 2-Hydroxybenzoylhydrazine (936-02-7) → N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide (1607483-32-8)

Guidance literature:

In methanol; for 1h; Reflux;

DOI:10.1080/15533174.2013.778883

Reference yield: 67.0%

bis(acetylacetonato)dioxidomolybdenum(VI) + N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide (1607483-32-8) → C15H13BrMoN2O6

Guidance literature:

In methanol; for 1h; Reflux;

DOI:10.1080/15533174.2013.778883

Reference yield: 55.0%

methanol (67-56-1) + bis(acetylacetonate)oxidovanadium(IV) + N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide (1607483-32-8) → [VO(N'-(3-bromo-2-hydroxybenzylidene)-2-hydroxybenzohydrazide(-2H))(OCH3)(methanol)]

Guidance literature:

for 1h; Reflux;

DOI:10.1080/15533174.2013.862810

upstream raw materials:

2-hydroxy-3-bromobenzaldehyde

2-Hydroxybenzoylhydrazine