Potassium dimethyldithiocarbamate

Base Information

• Chemical Name: Potassium dimethyldithiocarbamate
• CAS No.: 128-03-0
• Molecular Formula: C3H6KNS2
• Molecular Weight: 159.318
• Hs Code.: 2930909090
• Mol file: 128-03-0.mol

Synonyms:Carbamicacid, dimethyldithio-, potassium salt (8CI);Carbamodithioic acid, dimethyl-,potassium salt (9CI);Arylane;Busan 85;MBC 350;PotassiumN,N-dimethyldithiocarbamate;

Chemical Property of Potassium dimethyldithiocarbamate

Chemical Property:

• Appearance/Colour: clear light amber liquid
• Vapor Pressure: 0-0Pa at 20-25℃
• Melting Point: <0°C
• Boiling Point: 129.4 °C at 760 mmHg
• Flash Point: 32 °C
• PSA: 60.63000
• Density: 1.23-1.51 at 20℃
• LogP: 1.03040

Purity/Quality:

99% ^*data from raw suppliers

Busan85 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): N
• Hazard Codes: N
• Statements: 50
• Safety Statements: 61

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of Potassium dimethyldithiocarbamate

There total 1 articles about Potassium dimethyldithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + dimethyl amine (124-40-3) → potassium dimethyldithiocarbamate (128-03-0)

Guidance literature:

With potassium hydroxide; In ethanol; for 1h; Ambient temperature;

DOI:10.1016/0223-5234(96)89561-4

Reference yield: 95.0%

potassium dimethyldithiocarbamate (128-03-0) + [2-(2-chloro-2-phenyl-acetylamino)-thiazol-4-yl]-acetic acid ethyl ester (294886-87-6) → [2-(2-dimethylthiocarbamoylsulfanyl-2-phenyl-acetylamino)-thiazol-4-yl]-acetic acid ethyl ester

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1002/ardp.200390002

Reference yield: 80.0%

Co(C5H5)(C(CH3)NCH2C6H5)(P(CH3)2C6H5)(1+)*I(1-) = [Co(C5H5)(C(CH3)NCH2C6H5)(P(CH3)2C6H5)]I + potassium dimethyldithiocarbamate (128-03-0) → [Co(C5H5)(SC(S)N(CH2C6H5)C(CH2))(P(CH3)2C6H5)]

Guidance literature:

In dichloromethane; byproducts: KI, HNMe2; (argon); stirring (room temp., 4 h); solvent removal, redissoln. (CH2Cl2), chromy. (Al2O3; CH2Cl2/pentane), evapn., recrystn. (CH2Cl2/Et2O); elem. anal.;

DOI:10.1002/cber.19971300710

upstream raw materials:

carbon disulfide

dimethyl amine

Downstream raw materials:

dimethylthiocarbamoylsulfanyl-phenyl-acetic acid

diphenamid

N,N-di-methyl-tert-butylsulfenyl dithiocarbamate

Dithiokohlensaeure-S-benzoyloxymethylester-dimethylamid

Refernces

• 1、 Kapanda, Coco N.,Muccioli, Giulio G.,Labar, Geoffray,Poupaert, Jacques H.,Lambert, Didier M.. "Bis(dialkylaminethiocarbonyl)disulfides as potent and selective monoglyceride lipase inhibitors". experimental part. p. 7310 - 7314. Retrieved 2010/07/14.