3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

Base Information

Chemical Name:3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine
CAS No.:1616560-41-8
Molecular Formula:C₂₁H₂₄N₂O
Molecular Weight:320.434
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

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Technology Process of 3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

There total 3 articles about 3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1616560-22-5
1-(1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-ylidene)-2-phenylhydrazine

: 1616560-41-8
3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In N,N-dimethyl-formamide; at 130 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c4ob00839a

Reference yield:

: 32097-05-5
4-methoxy-β,β-dimethylacrylophenone

: 1616560-41-8
3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: titanium tetrachloride / dichloromethane / -78 °C

1.2: 0.58 h / 20 °C

2.1: acetic acid / ethanol / 60 °C / Inert atmosphere

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / N,N-dimethyl-formamide / 4 h / 130 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; titanium tetrachloride; acetic acid; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4ob00839a

Reference yield:

: 1616560-09-8
1-(4-methoxyphenyl)-3,3-dimethylhex-5-en-1-one

: 100-63-0
phenylhydrazine

: 1616560-41-8
3-(4-methoxyphenyl)-5,5-dimethyl-1-phenyl-6-vinyl-1,4,5,6-tetrahydropyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 60 °C / Inert atmosphere

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / N,N-dimethyl-formamide / 4 h / 130 °C / Inert atmosphere

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c4ob00839a