ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

Base Information

Chemical Name:ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride
CAS No.:1372860-85-9
Molecular Formula:C₁₃H₁₆Cl₂N₂O₄*ClH
Molecular Weight:371.648
Hs Code.:

Synonyms:ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

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Chemical Property of ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

Chemical Property:

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Technology Process of ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

There total 4 articles about ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl 2-{[(2,3-dichloro-6-nitrophenyl)methylidene]amino}-2-methylpropanoate hydrochloride

: 1372860-85-9
ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

Guidance literature:: With sodium tetrahydroborate; acetic acid; In toluene; at 0 - 30 ℃; for 13.5833h; Industry scale;

Reference yield:

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 1372860-85-9
ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 3.5 h / 20 - 44 °C / Industry scale

1.2: 4 h / 16 - 28 °C

2.1: triethylamine / toluene / 8.92 h / 17 - 110 °C / Industry scale

3.1: sodium tetrahydroborate; acetic acid / toluene / 13.58 h / 0 - 30 °C / Industry scale

With sodium tetrahydroborate; sulfuric acid; acetic acid; triethylamine; In toluene;

Reference yield:

: 17288-15-2
ethyl 2-aminoisobutyrate hydrochloride

: 1372860-85-9
ethyl 2-[(2,3-dichloro-6-nitrobenzyl)amino]isobutyrate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene / 8.92 h / 17 - 110 °C / Industry scale

2: sodium tetrahydroborate; acetic acid / toluene / 13.58 h / 0 - 30 °C / Industry scale

With sodium tetrahydroborate; acetic acid; triethylamine; In toluene;