Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

Base Information

Chemical Name:Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside
CAS No.:136773-78-9
Molecular Formula:C₁₉H₂₅NO₈S
Molecular Weight:427.475
Hs Code.:

Synonyms:Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

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Chemical Property of Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

Chemical Property:

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Technology Process of Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

There total 4 articles about Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63064-49-3,65947-37-7,74984-83-1,74984-84-2,88903-98-4,92841-84-4,116347-88-7,136845-44-8,138456-61-8
N-((2R,4aR,7R,8R,8aS)-6-(allyloxy)-8-hydroxy-2-phenylhexahydropyrano[3,2-d][1,3]dioxin-7-yl)acetamide

: 124-63-0
methanesulfonyl chloride

: 136773-78-9,137344-93-5
Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

Guidance literature:: With triethylamine; at 24 ℃; for 0.833333h; Yield given;
DOI:10.1002/hlca.19910740625

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 136773-78-9,137344-93-5
Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / BF₃*Et₂O / 4.5 h / 95 °C

2: 49 percent / ZnCl₂ / 19 h / Ambient temperature

3: NEt₃ / 0.83 h / 24 °C

With boron trifluoride diethyl etherate; triethylamine; zinc(II) chloride;
DOI:10.1002/hlca.19910740625

Reference yield:

: 100-52-7
benzaldehyde

: 136773-78-9,137344-93-5
Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(methanesulfonyl)-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / ZnCl₂ / 19 h / Ambient temperature

2: NEt₃ / 0.83 h / 24 °C

With triethylamine; zinc(II) chloride;
DOI:10.1002/hlca.19910740625