divanillyl disulfide

Base Information

• Chemical Name: divanillyl disulfide
• CAS No.: 7484-07-3
• Molecular Formula: C₁₆H₁₈O₄S₂
• Molecular Weight: 338.449
• Mol file: 7484-07-3.mol

Synonyms:divanillyl disulfide

Chemical Property of divanillyl disulfide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of divanillyl disulfide

There total 5 articles about divanillyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

4-hydroxymethyl-2-methoxyphenol (498-00-0) → bis-(4-hydroxy-3-methoxyphenyl)methane (3888-22-0) + 4,4'-[thiobis(methylene)]bis(2-methoxyphenol) (7452-87-1) + divanillyl disulfide (7484-07-3) + 4-hydroxy-3-methoxybenzenemethanthiol

Guidance literature:

4-hydroxymethyl-2-methoxyphenol; With hydrogenchloride; thiourea; In tetrahydrofuran; water; at 20 - 55 ℃; for 1h;

With sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 4h;

DOI:10.1021/acs.jafc.5b05733

Reference yield: 30.0%

vanillin (121-33-5,8014-42-4) → divanillyl disulfide (7484-07-3)

Guidance literature:

With sodium hydrogen sulfide; In ethanol; water; at 20 - 60 ℃;

DOI:10.1021/acs.jafc.5b05733

Reference yield:

4-hydroxymethyl-2-methoxyphenol (498-00-0) → divanillyl disulfide (7484-07-3)

Guidance literature:

With sodium sulfide;

upstream raw materials:

4-hydroxymethyl-2-methoxyphenol

vanillin

Downstream raw materials:

diveratryl disulfide