ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

Base Information

Chemical Name:ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate
CAS No.:109308-97-6
Molecular Formula:C₁₄H₁₃Cl₂FN₂O₄
Molecular Weight:363.173
Hs Code.:

Synonyms:ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

There total 2 articles about ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 704-10-9
2,4-dichloro-5-fluoroacetophenone

: 109308-97-6
ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaH / 1.5 h / 80 °C

2: 1) acetic anhydride / 1) 130 deg C, 1.5 h; 2) CH₂Cl₂, 1.5 h

With acetic anhydride; sodium hydride;
DOI:10.1002/jhet.5570220421

Reference yield:

: 758-17-8
1-Methyl-1-formylhydrazid

: 86483-51-4
ethyl 2,4-dichloro-5-fluoro-benzoyl-acetate

: 122-51-0
orthoformic acid triethyl ester

: 109308-97-6
ethyl 3-N-formyl-N-methylhydrazyl-2-(2,4-dichloro-5-fluoro)benzoylacrylate

Guidance literature:: With acetic anhydride; Yield given. Multistep reaction; 1) 130 deg C, 1.5 h; 2) CH₂Cl₂, 1.5 h;
DOI:10.1002/jhet.5570220421