Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

Base Information

Chemical Name:Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester
CAS No.:128970-60-5
Molecular Formula:C₉H₆ClIO₂
Molecular Weight:308.503
Hs Code.:

Synonyms:Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

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Chemical Property of Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

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Technology Process of Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

There total 2 articles about Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-18-6
formic acid

: 1483-82-5
phenylethynyl chloride

: 128970-60-5
Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

Guidance literature:: With tetrafluoroboric acid diethyl ether; Barluenga reagent; In dichloromethane; water; for 14h; Ambient temperature;
DOI:10.1016/S0040-4039(00)94690-2

Reference yield:

: 536-74-3
phenylacetylene

: 128970-60-5
Formic acid (E)-2-chloro-2-iodo-1-phenyl-vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) LiAlH₄, 2) N-chlorosuccinimide / 1) THF, RT, 1h, 2) 30 min

2: 90 percent / IPy₂BF₄, HBF₄*OEt₂ / CH₂Cl₂; H₂O / 14 h / Ambient temperature

With tetrafluoroboric acid diethyl ether; N-chloro-succinimide; lithium aluminium tetrahydride; Barluenga reagent; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)94690-2