2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

Base Information

Chemical Name:2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester
CAS No.:1415920-62-5
Molecular Formula:C₂₂H₁₇F₅N₂O₆
Molecular Weight:500.379
Hs Code.:

Synonyms:2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

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Chemical Property of 2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

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Technology Process of 2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

There total 6 articles about 2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1024602-85-4
2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetic acid

: 1415920-62-5
2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 3 - 22 ℃; for 18h;
DOI:10.1021/op4002998

Reference yield:

: 16642-79-8
3-(4-nitrophenyl)propionic acid

: 1415920-62-5
2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / toluene / 20 °C

2: n-butyllithium / tetrahydrofuran / -78 - 20 °C

3: hydrogen; hydrogenchloride; palladium on activated charcoal / methanol / 35 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

5: diisopropyl-carbodiimide / tetrahydrofuran / 20 °C

With hydrogenchloride; n-butyllithium; thionyl chloride; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.11.104

Reference yield:

: 107324-93-6
3-(p-nitrophenyl)propanoyl chloride

: 1415920-62-5
2-(2-oxo-2-(4-(3-oxo-3-(2-oxoazetidin-1-yl)propyl)phenylamino)ethoxy)acetate pentafluorophenol ester

Guidance literature:: Multi-step reaction with 4 steps

1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2: hydrogen; hydrogenchloride; palladium on activated charcoal / methanol / 35 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

4: diisopropyl-carbodiimide / tetrahydrofuran / 20 °C

With hydrogenchloride; n-butyllithium; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.104