5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

Base Information

Chemical Name:5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide
CAS No.:1401803-67-5
Molecular Formula:C₂₄H₂₇ClN₄O₄S
Molecular Weight:503.022
Hs Code.:

Synonyms:5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

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Chemical Property of 5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

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Technology Process of 5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

There total 3 articles about 5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₁Cl₂N₃O₃S

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1401803-67-5
5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 162758-34-1
ethyl [2-acetyl-4-(4-chlorophenyl)-3-methyl-4-oxo]butyrate

: 1401803-67-5
5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 17 h / 95 °C

2.1: sodium hydroxide; water / ethanol / 3 h / Reflux

2.2: pH <= 7

3.1: oxalyl dichloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; water; acetic acid; triethylamine; sodium hydroxide; In ethanol; dichloromethane;

Reference yield:

: 1401803-66-4
5-(4-chlorophenyl)-2,4-dimethyl-1-(4-sulfamoylphenyl)-1H-pyrrole-3-carboxylic acid

: 1401803-67-5
5-(4-chlorophenyl)-1-(4-(N-((dimethylamino)methylene)sulfamoyl)phenyl)-N-methoxy-N,2,4-trimethyl-1H-pyrrole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In dichloromethane;