(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

Base Information

Chemical Name:(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester
CAS No.:80453-93-6
Molecular Formula:C₂₀H₂₄O₅
Molecular Weight:344.408
Hs Code.:

Synonyms:(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

Suppliers and Price of (2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

Chemical Property:

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Technology Process of (2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

There total 1 articles about (2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 63826-41-5
2E,4E,6E-2,6-Dimethyl-7-ethoxycarbonyl-2,4,6-heptatrienal

: 80453-93-6
(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

Guidance literature:: Yield given. Multistep reaction; 1.) THF, 0 deg C, 2.) THF, -20 deg C;
DOI:10.1016/S0040-4039(01)81931-6

Reference yield: 85.0%

: 80453-93-6
(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

: 75-36-5
acetyl chloride

: 80453-89-0
(2E,4E,6E)-(8S,9R)-8-Acetoxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(01)81931-6

Reference yield:

: 80453-93-6
(2E,4E,6E)-(8R,9S)-8-Hydroxy-3,7-dimethyl-9-phenyl-deca-2,4,6-trienedioic acid 1-ethyl ester

: 66757-08-2
ethyl (2E,4E,6E,8E)-3,7-dimethyl-9-phenylnona-2,4,6,8-tetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / C₅H₅N / CH₂Cl₂ / 0 °C

2: 60 percent / (C₂H₅)3N / (Ph₃P)4Pd / tetrahydrofuran / Heating

With pyridine; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(01)81931-6