3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone

Base Information

• Chemical Name: 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone
• CAS No.: 397884-34-3
• Molecular Formula: C₁₈H₁₅ClN₄O₃
• Molecular Weight: 370.795

Synonyms:3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone

Chemical Property of 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone

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Technology Process of 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone

There total 1 articles about 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(4-carboxyphenylhydrazono)methyl-3-(4-methylphenyl)sydnone (86870-31-7) + α-chloroformyl-(4-methylphenyl)hydrazine hydrochloride → 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone (397884-34-3)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.5h;

DOI:10.1002/jccs.200100110

Reference yield: 82.0%

4-ethoxycarbonylphenylhydrazine (14685-90-6) + 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone (397884-34-3) → 3-(4-methylphenyl)sydnon-4-ylaldehyde 5-(4-ethoxycarbonylphenyl)-2-(4-methylphenyl)carbazone

Guidance literature:

With triethylamine; In ethanol; at 20 ℃; for 0.25h;

DOI:10.1002/jccs.200100110

Reference yield: 54.0%

4-fluorophenylhydrazine (371-14-2) + 3-(4-methylphenyl)sydnon-4-ylformaldehyde α-chloroformyl4-methylphenylhydrazone (397884-34-3) → 3-(4-methylphenyl)sydnon-4-ylaldehyde 5-(4-fluorophenyl)-2-(4-methylphenyl)carbazone + 2-(4-fluorophenyl)-4-(4-methylphenyl)-6-[3-(4-methylphenyl)sydnon-4-yl]-1,2,4,5-tetrazinan-3-one

Guidance literature:

With triethylamine; In ethanol; at 20 ℃; for 0.25h;

DOI:10.1002/jccs.200100110

upstream raw materials:

4-(4-carboxyphenylhydrazono)methyl-3-(4-methylphenyl)sydnone

Downstream raw materials:

2-(4-methylphenyl)-6-[3-(4-methylphenyl)sydnon-4-yl]-4-phenyl-1,2,4,5-tetrazinan-3-one

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