acetone-N-(4-methylbenzoyl)hydrazone

Base Information

• Chemical Name: acetone-N-(4-methylbenzoyl)hydrazone
• CAS No.: 92574-02-2
• Molecular Formula: C₁₁H₁₄N₂O
• Molecular Weight: 190.245
• Mol file: 92574-02-2.mol

Synonyms:acetone-N-(4-methylbenzoyl)hydrazone

Chemical Property of acetone-N-(4-methylbenzoyl)hydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of acetone-N-(4-methylbenzoyl)hydrazone

There total 1 articles about acetone-N-(4-methylbenzoyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

p-toluic hydrazide (3619-22-5) + acetone (67-64-1) → acetone-N-(4-methylbenzoyl)hydrazone (92574-02-2)

Guidance literature:

With sodium sulfate; at 20 ℃; for 18h;

DOI:10.1055/s-2005-869858

Reference yield: 92.0%

acetone-N-(4-methylbenzoyl)hydrazone (92574-02-2) → N'-isopropyl-4-methylbenzohydrazide

Guidance literature:

With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 18h;

DOI:10.1055/s-2005-869858

Reference yield: 55.0%

methanol (67-56-1) + acetone-N-(4-methylbenzoyl)hydrazone (92574-02-2) → 2-methoxy-5,5-dimethyl-2-(4-methylphenyl)-Δ3-1,3,4-oxadiazoline (92573-95-0)

Guidance literature:

With lead(IV) acetate; potassium hydroxide; for 2h;

upstream raw materials:

p-toluic hydrazide

acetone

Downstream raw materials:

2-methoxy-5,5-dimethyl-2-(4-methylphenyl)-Δ³-1,3,4-oxadiazoline

(E)-tert-butyl 3-(3-(1-isopropyl-2-(4-methylbenzoyl)hydrazinyl)-3-oxoprop-1-enyl)-1H-indole-1-carboxylate