bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

Base Information

Chemical Name:bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine
CAS No.:1203669-57-1
Molecular Formula:C₂₄H₂₈BN₃O₂
Molecular Weight:401.316
Hs Code.:

Synonyms:bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

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Technology Process of bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

There total 2 articles about bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1129527-13-4
(4-iodo-phenyl)-bis-pyridin-2-ylmethyl-amine

: 73183-34-3
bis(pinacol)diborane

: 1203669-57-1
bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

Guidance literature:: With potassium acetate; palladium diacetate; triphenylphosphine; In dimethyl sulfoxide; at 80 ℃; for 18h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1cc04122c

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1203669-57-1
bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / water / 96 h / 20 °C / Inert atmosphere; Schlenk technique

2: palladium diacetate; triphenylphosphine; potassium acetate / dimethyl sulfoxide / 18 h / 80 °C / Inert atmosphere; Schlenk technique

With potassium tert-butylate; potassium acetate; palladium diacetate; triphenylphosphine; In water; dimethyl sulfoxide;
DOI:10.1039/d1cc04122c

Reference yield: 63.0%

: 1203669-57-1
bis-pyridin-2-ylmethyl-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-phenyl]-amine

: 14658-95-8
1,3-dibromoazulene

: 4,4'-(azulene-1,3-diyl)bis(N,N-bis(2-picolyl)aniline)

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; In tetrahydrofuran; water; at 75 ℃; for 18h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1cc04122c