dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside
CAS No.:1198155-91-7
Molecular Formula:C₅₇H₆₉N₃O₁₆Si
Molecular Weight:1080.27
Hs Code.:

dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Synonyms:dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Suppliers and Price of dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

There total 6 articles about dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1198156-25-0
dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1198155-91-7
dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1021/acs.joc.0c01881

Reference yield:

: 1198157-07-1
dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

: 1198155-91-7
dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 6 h

2: methanol; toluene / 0.25 h

3: pyridine

With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In methanol; dichloromethane; water; toluene;
DOI:10.1021/acs.joc.0c01881

Reference yield:

: C₄₁H₅₇N₃O₁₄Si

: 1198155-91-7
dimethylthexylsilyl O-(methyl 2-O-acetyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; toluene / 0.25 h

2: pyridine

With pyridine; In methanol; toluene;
DOI:10.1021/acs.joc.0c01881