3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

Base Information

Chemical Name:3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol
CAS No.:215244-99-8
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

Synonyms:3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

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Chemical Property of 3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

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Technology Process of 3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

There total 8 articles about 3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid 3-(3-methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenyl ester

: 215244-99-8
3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

Guidance literature:: With sodium methylate; In methanol; for 0.5h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(98)01657-8

Reference yield:

: 2999-40-8
1,3,5-triacetoxybenzene

: 215244-99-8
3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / NaH / H₂O; dimethylformamide / 2.5 h / from 0 deg C to RT

2: 74 percent / NaOMe / methanol / 0.5 h / Ambient temperature

3: PPh₃, DIAD / tetrahydrofuran / 3 h / from 0 deg C to RT

4: NaOMe / methanol / 0.5 h / Ambient temperature

With di-isopropyl azodicarboxylate; sodium methylate; sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)01657-8

Reference yield:

: 69395-13-7
4-(2-hydroxyethyl)benzonitrile

: 215244-99-8
3-(3-Methyl-butoxy)-5-{2-[4-(5-methyl-[1,2,4]oxadiazol-3-yl)-phenyl]-ethoxy}-phenol

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / NH₂OH / methanol / 24 h / Ambient temperature

2: 82 percent / 4 h / 120 °C

3: 94 percent / NaOMe / methanol / 0.5 h / Ambient temperature

4: PPh₃, DIAD / tetrahydrofuran / 3 h / from 0 deg C to RT

5: NaOMe / methanol / 0.5 h / Ambient temperature

With di-isopropyl azodicarboxylate; hydroxylamine; sodium methylate; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(98)01657-8