2-((2-bromophenyl)amino)phenol

Base Information

• Chemical Name: 2-((2-bromophenyl)amino)phenol
• CAS No.: 1629168-52-0
• Molecular Formula: C₁₂H₁₀BrNO
• Molecular Weight: 264.121
• Mol file: 1629168-52-0.mol

Synonyms:2-((2-bromophenyl)amino)phenol

Chemical Property of 2-((2-bromophenyl)amino)phenol

Chemical Property:

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Technology Process of 2-((2-bromophenyl)amino)phenol

There total 1 articles about 2-((2-bromophenyl)amino)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

6-diazo-2-cyclohexen-1-one (928642-45-9) + 2-bromoaniline (615-36-1) → 2-((2-bromophenyl)amino)phenol (1629168-52-0)

Guidance literature:

With oxygen; copper diacetate; In 1,4-dioxane; at 80 ℃; for 8h; Schlenk technique; Sealed tube;

DOI:10.1002/asia.201402080

Reference yield: 55.0%

iodobenzene (591-50-4) + 2-((2-bromophenyl)amino)phenol (1629168-52-0) → 10-phenyl-10H-phenoxazine (37832-25-0)

Guidance literature:

With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 12h;

DOI:10.1039/c4ra09593f

upstream raw materials:

6-diazo-2-cyclohexen-1-one

2-bromoaniline

Downstream raw materials:

10-phenyl-10H-phenoxazine