benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

Base Information

Chemical Name:benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate
CAS No.:420797-67-7
Molecular Formula:C₂₀H₂₀F₃NO₆S
Molecular Weight:459.443
Hs Code.:

Synonyms:benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

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Chemical Property of benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

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Technology Process of benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

There total 6 articles about benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 762254-68-2
C₁₉H₂₁NO₄

: 358-23-6
trifluoromethylsulfonic anhydride

: 420797-67-7
benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 5-chlorocarbonyl-2-trifluoromethanesulfonyloxy-benzoic acid benzyl ester

: 78-81-9
isobutylamine

: 420797-67-7
benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.bmc.2006.08.010

Reference yield:

: 239462-58-9
benzyl 2-trifluoromethylsulfonyloxy-5-formylbenzoate

: 420797-67-7
benzyl 5-(isobutylamino)carbonyl-2-{[(trifluoromethyl)sulfonyl]oxy}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: NaH₂PO₄*H₂O; 2-methyl-2-butene; sodium chlorite / 2-methyl-propan-2-ol; H₂O; acetonitrile / 1 h / 20 °C

2: oxalyl chloride / CH₂Cl₂; dimethylformamide / 2 h / 20 °C

3: 2.89 g / triethylamine / CH₂Cl₂ / 1 h / 0 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.08.010