trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide

Base Information

• Chemical Name: trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide
• CAS No.: 28097-07-6
• Molecular Formula: C₅H₉Cl₂O₃P
• Molecular Weight: 219.004

Synonyms:trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide

Chemical Property of trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide

There total 3 articles about trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-4-phospha-3,5,8-trioxa-bicyclo<2,2,2>octane-4-sulfide (3196-56-3) → 4-methyl-2,6,7-trioxa-1-phosphabicyclo<2.2.2>octane 1-oxide (1449-89-4) + trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide (28097-07-6)

Guidance literature:

With sulfuryl dichloride; In dichloromethane;

Reference yield:

methanol (67-56-1) + (5-Chloromethyl-5-methyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-hydrazine (106019-48-1) → trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide (28097-07-6) + cis-2-chloro-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (21071-81-8) + cis-2-methoxy-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (28097-12-3) + trans-2-methoxy-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (36912-27-3)

Guidance literature:

With tert-butylhypochlorite; at 20 ℃; Product distribution;

DOI:10.1016/S0040-4039(01)01329-6

Reference yield:

methanol (67-56-1) + (5-Chloromethyl-5-methyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yl)-hydrazine (106019-47-0) → trans-2-chloro-5-methyl-1,3,2-dioxaphosphorinane-r-5-methyl chloride 2-oxide (28097-07-6) + cis-2-chloro-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (21071-81-8) + cis-2-methoxy-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (28097-12-3) + trans-2-methoxy-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane (36912-27-3)

Guidance literature:

With tert-butylhypochlorite; at 20 ℃; Product distribution;

DOI:10.1016/S0040-4039(01)01329-6

upstream raw materials:

1-methyl-4-phospha-3,5,8-trioxa-bicyclo<2,2,2>octane-4-sulfide

methanol

(5-Chloromethyl-5-methyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-hydrazine

(5-Chloromethyl-5-methyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yl)-hydrazine

Downstream raw materials:

trans-2-methoxy-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinane

5-Chloromethyl-5-methyl-2-phenoxy-[1,3,2]dioxaphosphinane 2-oxide

5-Chloromethyl-5-methyl-2-phenoxy-[1,3,2]dioxaphosphinane 2-oxide

trans-2-(p-Nitrophenyl)-5-(chloromethyl)-5-methyl-2-oxo-1,3,2-dioxaphosphorinan

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