2-(2-hydroxyphenyl)-6-methylbenzoxazole

Base Information

• Chemical Name: 2-(2-hydroxyphenyl)-6-methylbenzoxazole
• CAS No.: 60344-93-6
• Molecular Formula: C₁₄H₁₁NO₂
• Molecular Weight: 225.247

Synonyms:2-(2-hydroxyphenyl)-6-methylbenzoxazole

Chemical Property of 2-(2-hydroxyphenyl)-6-methylbenzoxazole

Chemical Property:

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Technology Process of 2-(2-hydroxyphenyl)-6-methylbenzoxazole

There total 11 articles about 2-(2-hydroxyphenyl)-6-methylbenzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Hydroxy-4-methylanilin (2835-98-5) + 4-chloro-2,2-dimethyl-2H-benzo[e][1,3]oxazine (74405-07-5) → 2-(2-hydroxyphenyl)-6-methylbenzoxazole (60344-93-6)

Guidance literature:

In acetonitrile; for 1h; Heating;

Reference yield: 72.0%

6-methyl-2-phenylbenzoxazole (14016-00-3) → 2-(2-hydroxyphenyl)-6-methylbenzoxazole (60344-93-6)

Guidance literature:

With sodium persulfate; palladium diacetate; In 1,4-dioxane; at 80 ℃; for 14h; Inert atmosphere;

DOI:10.1039/c4cc06864e

Reference yield: 52.0%

2-methyl-benzyl alcohol (89-95-2) + 2-Hydroxy-4-methylanilin (2835-98-5) → 2-(2-hydroxyphenyl)-6-methylbenzoxazole (60344-93-6)

Guidance literature:

With lead(IV) acetate; acetic acid; for 1h;

DOI:10.1021/ja047815i

upstream raw materials:

7-methyldibenzo[b,f ][1,4]oxazepine

2-Hydroxy-4-methylanilin

4-chloro-2,2-dimethyl-2H-benzo[e][1,3]oxazine

2-methyl-benzyl alcohol

Downstream raw materials:

acetic acid 2-(6-methyl-benzooxazol-2-yl)-phenyl ester

2-(2-hydroxyphenyl)benzo[d]oxazole-6-carbaldehyde

acetic acid 2-(6-bromomethylbezoxazol-2-yl)phenyl ester

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