(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Base Information

Chemical Name:(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine
CAS No.:85879-93-2
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:

Synonyms:(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Suppliers and Price of (E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Chemical Property:

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Technology Process of (E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

There total 6 articles about (E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 2026-48-4,473-75-6
(S)-valinol

: 123-11-5
4-methoxy-benzaldehyde

: 85879-93-2
(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Guidance literature:: In benzene; for 4h; Heating;
DOI:10.1248/cpb.30.3160

Reference yield:

: 2026-48-4,473-75-6
(S)-valinol

: 26227-73-6
N-(4-methoxybenzylidene)-4-(n-butyl)aniline

: 104-13-2
4-Butylaniline

: 85879-93-2
(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Guidance literature:: In dichloromethane; for 12h; Ambient temperature;
DOI:10.1021/jo00161a005

Reference yield:

: 609-12-1
ethyl 2-bromoisovalerate

: 85879-93-2
(E)-(S)-(-)-N-(2-hydroxy-1-isopropylethyl)p-methoxyphenylmethylideneamine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / lithium aluminium hydride / diethyl ether / 1 h

2: 67 percent / anh. Na₂CO₃ / ethanol / 18 h / Heating

3: H₂, cc. HCl / 10percent Pd-C / methanol / 4045.3 Torr

4: 74 percent / benzene / 4 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; diethyl ether; ethanol; benzene;
DOI:10.1248/cpb.30.3160