C₃₀H₃₉⁽²⁾HN₂O₆Si

Base Information

Chemical Name:C₃₀H₃₉⁽²⁾HN₂O₆Si
CAS No.:203510-18-3
Molecular Formula:C₃₀H₄₀N₂O₆Si
Molecular Weight:553.735
Hs Code.:

C<sub>30</sub>H<sub>39</sub><sup>(2)</sup>HN<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₀H₃₉⁽²⁾HN₂O₆Si

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Chemical Property of C₃₀H₃₉⁽²⁾HN₂O₆Si

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Technology Process of C₃₀H₃₉⁽²⁾HN₂O₆Si

There total 9 articles about C₃₀H₃₉⁽²⁾HN₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 203510-16-1
C₂₄H₂₅⁽²⁾HN₂O₆

: 203510-18-3
C₃₀H₃₉⁽²⁾HN₂O₆Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)10815-2

Reference yield:

: 34311-63-2
5-O-benzyl-3-oxo-1,2-O-isopropylidene-α-D-xylofuranose

: 203510-18-3
C₃₀H₃₉⁽²⁾HN₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: NaB⁽²⁾H₄ / ethanol

2: NaH / dimethylformamide

3: TsOH / dioxane; H₂O

4: pyridine; acetonitrile

5: 88 percent / bis(trimethylsilylacetamide), SnCl₄ / acetonitrile

6: 85 percent / NH₃ / methanol

7: 100 percent / imidazole / dimethylformamide

With 1H-imidazole; sodium borodeuteride; bis(trimethylsilylacetamide); ammonia; tin(IV) chloride; sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; pyridine; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)10815-2

Reference yield:

: 100-39-0
benzyl bromide

: 203510-18-3
C₃₀H₃₉⁽²⁾HN₂O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) (Bu₃Sn)2O; 2.) Bu₄NI; 3.) triacetoxy periodinane / 1.) toluene; 2.) toluene

2: NaB⁽²⁾H₄ / ethanol

3: NaH / dimethylformamide

4: TsOH / dioxane; H₂O

5: pyridine; acetonitrile

6: 88 percent / bis(trimethylsilylacetamide), SnCl₄ / acetonitrile

7: 85 percent / NH₃ / methanol

8: 100 percent / imidazole / dimethylformamide

With 1H-imidazole; sodium borodeuteride; bis(trimethylsilylacetamide); ammonia; tin(IV) chloride; tetra-(n-butyl)ammonium iodide; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; bis(tri-n-butyltin)oxide; In 1,4-dioxane; pyridine; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(97)10815-2