methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate

Base Information

• Chemical Name: methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate
• CAS No.: 121766-30-1
• Molecular Formula: C₁₇H₁₉NO₄
• Molecular Weight: 301.342
• Mol file: 121766-30-1.mol

Synonyms:methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate

Chemical Property of methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate

There total 8 articles about methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

(4-methoxy-phenyl)-(4-methoxy-phenylimino)-acetic acid methyl ester → methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate (121766-30-1)

Guidance literature:

With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; iodine; In dichloromethane; at 20 ℃; for 24h; chemoselective reaction; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.05.071

Reference yield: 55.0%

(E)-1,N-bis(4-methoxyphenyl)methanimine (1624-46-0,1749-08-2,83306-67-6) + methyl 1-imidazolecarboxylate (61985-23-7) → methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate (121766-30-1)

Guidance literature:

With chloro-trimethyl-silane; tert-butylammonium hexafluorophosphate(V); triethylamine; In tetrahydrofuran; at 20 ℃; Electrolysis;

DOI:10.1016/j.tet.2007.11.106

Reference yield:

methyl 2-diazo-2-(4-methoxypheny)acetate (22979-36-8) + 4-methoxy-aniline (104-94-9) → methyl 2-(4-methoxyphenyl)-2-((4-methoxyphenyl)amino)acetate (121766-30-1)

Guidance literature:

With dirhodium tetraacetate; 1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In dichloromethane; at 45 ℃; for 1h;

DOI:10.1002/anie.202102506

upstream raw materials:

methanol

3,4-Bis-(4-methoxy-phenyl)-oxazolidine-2,5-dione

N-(4-methoxy benzylidene)-4-methoxyaniline

1,4-bis(4-methoxyphenyl)azetidine-2,3-dione