Technology Process of (S)-2-((S)-1-tert-Butoxycarbonyl-ethylamino)-decanoic acid benzyl ester; compound with (Z)-but-2-enedioic acid
There total 6 articles about (S)-2-((S)-1-tert-Butoxycarbonyl-ethylamino)-decanoic acid benzyl ester; compound with (Z)-but-2-enedioic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93.1 percent / benzene / 6 h / Heating
2: 37.9 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
3: ethyl acetate; diisopropyl ether
With
potassium carbonate;
In
di-isopropyl ether; dimethyl sulfoxide; ethyl acetate; benzene;
DOI:10.1021/jm00122a003
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92.1 percent
2: 47.5 percent / CoCl2 / H2O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7
3: 93.1 percent / benzene / 6 h / Heating
4: 37.9 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
5: ethyl acetate; diisopropyl ether
With
potassium carbonate;
In
di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate; benzene;
DOI:10.1021/jm00122a003
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 62.9 percent / 28percent aq. NH3 / 168 h / Ambient temperature
2: 92.1 percent
3: 47.5 percent / CoCl2 / H2O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7
4: 93.1 percent / benzene / 6 h / Heating
5: 37.9 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
6: ethyl acetate; diisopropyl ether
With
ammonium hydroxide; potassium carbonate;
In
di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate; benzene;
DOI:10.1021/jm00122a003
