Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene

Base Information

• Chemical Name: Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene
• CAS No.: 128364-57-8
• Molecular Formula: C₁₆H₁₇BrN₂O
• Molecular Weight: 333.228
• Mol file: 128364-57-8.mol

Synonyms:Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene

Chemical Property of Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene

There total 3 articles about Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

methanol (67-56-1) + N-Benzyl-N'-[1-(2-bromo-phenyl)-eth-(Z)-ylidene]-hydrazine (128364-48-7,128364-49-8) → Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene (128364-57-8)

Guidance literature:

With lead(IV) acetate;

DOI:10.1139/v90-088

Reference yield:

2-bromophenyl methyl ketone (2142-69-0) → Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene (128364-57-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / diethyl ether / Heating

2: 45 percent / lead tetraacetate

With lead(IV) acetate; In diethyl ether;

DOI:10.1139/v90-088

Reference yield:

Benzylhydrazine (555-96-4) → Benzyl-[1-(2-bromo-phenyl)-1-methoxy-ethyl]-diazene (128364-57-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / diethyl ether / Heating

2: 45 percent / lead tetraacetate

With lead(IV) acetate; In diethyl ether;

DOI:10.1139/v90-088

upstream raw materials:

methanol

N-Benzyl-N'-[1-(2-bromo-phenyl)-eth-(Z)-ylidene]-hydrazine

2-bromophenyl methyl ketone

Benzylhydrazine

Downstream raw materials:

1-benzyl-3-methyl-1H-indazole

Benzyl-(1-methoxy-1-phenyl-ethyl)-diazene

Refernces