4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

Base Information

Chemical Name:4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene
CAS No.:260045-58-7
Molecular Formula:C₁₂H₁₉N₃O₃
Molecular Weight:253.301
Hs Code.:

Synonyms:4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

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Chemical Property of 4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

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Technology Process of 4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

There total 1 articles about 4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 124-40-3
dimethyl amine

: 100-15-2
N-methyl(p-nitroaniline)

: 3132-64-7,82584-73-4
1,2-Epoxy-3-bromopropane

: 260045-58-7
4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

Guidance literature:: N-methyl(p-nitroaniline); With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.5h;

1,2-Epoxy-3-bromopropane; In DMF (N,N-dimethyl-formamide); at 18 - 25 ℃; for 12h;

dimethyl amine; In methanol; at 18 - 25 ℃; for 12h;

Reference yield: 60.0%

: 260045-58-7
4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene

: 4-[3-N,N-dimethylamino-2-hydroxypropyl-(N-methyl)amino]aniline hydrochloride

Guidance literature:: 4-{N-[2-hydroxy-3-(N,N-dimethylamino)propyl]-N-methylamino}nitrobenzene; With hydrogen; 10% palladium on activated carbon; In ethanol; for 3h;

With hydrogenchloride; In diethyl ether; dichloromethane;