5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole

Base Information

• Chemical Name: 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole
• CAS No.: 77722-47-5
• Molecular Formula: C₁₇H₁₂ClN₃O₂S
• Molecular Weight: 357.82
• Mol file: 77722-47-5.mol

Synonyms:5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole

Chemical Property of 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole

There total 3 articles about 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-chlorobenzenediazonium chloride (2028-74-2) → 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole (77722-47-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate / ethanol / 10 h / 0 °C

2: pyridine / 0.5 h / Heating

With sodium acetate; In pyridine; ethanol;

Reference yield:

2-oxo-N-(4-chlorophenyl)propanehydrazonoyl chloride (18247-78-4,1338563-31-7) → 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole (77722-47-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 5 h / Ambient temperature

2: pyridine / 0.5 h / Heating

In pyridine; ethanol;

Reference yield:

benzoyl chloride (98-88-4) + 5-acetyl-3-(4-chlorophenyl)-2-imino-1,3,4-thiadiazole (71687-14-4) → 5-acetyl-3-(4-chlorophenyl)-2-benzoylimino-3H-[1,3,4]thiadiazole (77722-47-5)

Guidance literature:

In pyridine; for 0.5h; Yield given; Heating;

upstream raw materials:

benzoyl chloride

5-acetyl-3-(4-chlorophenyl)-2-imino-1,3,4-thiadiazole

2-oxo-N-(4-chlorophenyl)propanehydrazonoyl chloride

p-chlorobenzenediazonium chloride

Downstream raw materials:

C₂₀H₁₇ClN₄O₂S

5-[2-benzoylimino-3-(4-chlorophenyl)-1,3,4-thiadiazol-5-yl]-[1,2,4]triazolo[1,5-a]pyrimidine

4-[2-benzoylimino-3-(4-chlorophenyl)-1,3,4-thiadiazol-5-yl]-benzimidazo[1,2-a]pyrimidine

N-[3-(4-chlorophenyl)-5-(1H-pyrazol-3-yl)-3H-[1,3,4]thiadiazol-2-ylidene]-benzamide