(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

Base Information

Chemical Name:(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester
CAS No.:129175-80-0
Molecular Formula:C₁₈H₂₂F₃N₃O₆
Molecular Weight:433.384
Hs Code.:

Synonyms:(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

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Chemical Property of (S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

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Technology Process of (S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

There total 4 articles about (S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129175-84-4
(S)-2-[4-Nitro-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

: 129175-80-0
(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h; under 760 Torr;
DOI:10.1021/jm00173a026

Reference yield:

: 1118-89-4
diethyl-L-glutamate hydrochloride

: 129175-80-0
(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1 h

2: H₂ / 10percent Pd/C / ethyl acetate / 4 h / 760 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00173a026

Reference yield:

: 91533-09-4
4-nitro-2-trifluoro-acetamido-benzoic acid

: 129175-80-0
(S)-2-[4-Amino-2-(2,2,2-trifluoro-acetylamino)-benzoylamino]-pentanedioic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 3 h

2: Et₃N / CH₂Cl₂ / 1 h

3: H₂ / 10percent Pd/C / ethyl acetate / 4 h / 760 Torr

With oxalyl dichloride; hydrogen; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00173a026