2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide

Base Information

• Chemical Name: 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide
• CAS No.: 169280-17-5
• Molecular Formula: C₁₆H₂₂ClNO₂
• Molecular Weight: 295.809

Synonyms:2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide

Chemical Property of 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide

Chemical Property:

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Technology Process of 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide

There total 2 articles about 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

tert-butylmethyl ether (28509-24-2) + 2-methyl-2-phenylpropionic acid (826-55-1) + N,N-dimethylammonium chloride (506-59-2) → 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide (169280-17-5) + 2-methyl-2-phenyl-propionic acid , dimethylamide (121800-25-7)

Guidance literature:

With hydrogenchloride; thionyl chloride; potassium carbonate; In water; toluene;

Reference yield: 72.0%

2-methyl-2-phenyl-propionic acid , dimethylamide (121800-25-7) + 4-Chlorobutanoyl chloride (4635-59-0) → 2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide (169280-17-5)

Guidance literature:

With aluminium trichloride; In tetrachloromethane; at 20 ℃; for 17h;

Reference yield: 63.0%

2-[4-(4-Chloro-butyryl)-phenyl]-2-methyl-propionic acid , dimethylamide (169280-17-5) + C18H21NO (115-46-8) → N,N-dimethyl-2-(4-{4-[4-(hydroxy-diphenylmethyl)-piperidin-1-yl]-butyryl}-phenyl)-isobutyramide (343255-27-6)

Guidance literature:

With potassium hydrogencarbonate; In water; xylene; at 100 ℃; for 20h; Heating / reflux;

upstream raw materials:

2-methyl-2-phenyl-propionic acid , dimethylamide

4-Chlorobutanoyl chloride

tert-butylmethyl ether

2-methyl-2-phenylpropionic acid

Downstream raw materials:

N,N-dimethyl-2-(4-{4-[4-(hydroxy-diphenylmethyl)-piperidin-1-yl]-butyryl}-phenyl)-isobutyramide

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