N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide
CAS No.:213685-55-3
Molecular Formula:C₂₅H₃₁N₃O₄S
Molecular Weight:469.605
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

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Technology Process of N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

There total 4 articles about N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 101495-34-5
4-nitrobenzo[d]oxazole-2-thiol

: 199592-72-8
6-bromo-N-(2,6-diisopropylphenyl)hexanamide

: 213685-55-3
N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 603-85-0
2-Amino-3-nitrophenol

: 213685-55-3
N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 - 60 °C

1.2: 0.08 h / 20 - 60 °C

2.1: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

With 18-crown-6 ether; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 213685-55-3
N-(2,6-diisopropylphenyl)-6-((4-nitrobenzo[d]oxazol-2-yl)thio)hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

With 18-crown-6 ether; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.06.024