3-(benzyloxy)-5-chloroisonicotinic acid

Base Information

Chemical Name:3-(benzyloxy)-5-chloroisonicotinic acid
CAS No.:1253799-61-9
Molecular Formula:C₁₃H₁₀ClNO₃
Molecular Weight:263.68
Hs Code.:

Synonyms:3-(benzyloxy)-5-chloroisonicotinic acid

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Chemical Property of 3-(benzyloxy)-5-chloroisonicotinic acid

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Technology Process of 3-(benzyloxy)-5-chloroisonicotinic acid

There total 1 articles about 3-(benzyloxy)-5-chloroisonicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 13958-93-5
3,5-dichloropyridine-4-carboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 1253799-61-9
3-(benzyloxy)-5-chloroisonicotinic acid

Guidance literature:: 3,5-dichloropyridine-4-carboxylic acid; With sodium hydride; In 1-methyl-pyrrolidin-2-one; mineral oil;

benzyl alcohol; In 1-methyl-pyrrolidin-2-one; mineral oil; at 20 - 80 ℃;

With hydrogenchloride; In 1-methyl-pyrrolidin-2-one; water; mineral oil; pH=2;

Reference yield: 88.0%

: 1253799-61-9
3-(benzyloxy)-5-chloroisonicotinic acid

: 108-95-2,27073-41-2
phenol

: 1253799-63-1
phenyl 3-(benzyloxy)-5-chloroisonicotinate

Guidance literature:: 3-(benzyloxy)-5-chloroisonicotinic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;

phenol; With dmap; triethylamine; In dichloromethane; for 1h;