2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Base Information

Chemical Name:2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime
CAS No.:134183-05-4
Molecular Formula:C₁₀H₅Cl₂F₃N₄O
Molecular Weight:325.077
Hs Code.:

Synonyms:2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Suppliers and Price of 2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

There total 3 articles about 2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2-Oxopropanedial 1-(O-acetyloxime) 2-(2,6-dichloro-4-trifluoromethylphenylhydrazone) 3-oxime

: 134183-05-4
2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Guidance literature:: With caesium carbonate; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1002/(SICI)1096-9063(199610)48:2<189::AID-PS461>3.0.CO;2-#

Reference yield:

: 86398-94-9
2,6-dichloro-4-(trifluoromethyl)phenyl hydrazine

: 134183-05-4
2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 2 h / Heating

2: 95 percent / AcOH / 0.75 h / 20 °C

3: 82 percent / Cs₂CO₃ / tetrahydrofuran / 1 h / 20 °C

With caesium carbonate; acetic acid; In tetrahydrofuran; 1: Condensation / 2: Acetylation / 3: Cyclization;
DOI:10.1002/(SICI)1096-9063(199610)48:2<189::AID-PS461>3.0.CO;2-#

Reference yield:

: 134183-03-2
2-Oxopropanedial 2-(2,6-dichloro-4-trifluoromethylphenylhydrazone) 1,3-dioxime

: 134183-05-4
2-(2,6-Dichloro-4-trifluoromethylphenyl)-2H-1,2,3-triazole-4-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / AcOH / 0.75 h / 20 °C

2: 82 percent / Cs₂CO₃ / tetrahydrofuran / 1 h / 20 °C

With caesium carbonate; acetic acid; In tetrahydrofuran; 1: Acetylation / 2: Cyclization;
DOI:10.1002/(SICI)1096-9063(199610)48:2<189::AID-PS461>3.0.CO;2-#