N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

Base Information

Chemical Name:N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide
CAS No.:1613039-83-0
Molecular Formula:C₁₄H₁₈N₄O₂
Molecular Weight:274.323
Hs Code.:

Synonyms:N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

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Chemical Property of N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

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Technology Process of N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

There total 3 articles about N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 57497-39-9
N-tertbutylhydroxylamine hydrochloride

: 133902-64-4
1-(4-methoxyphenyl)-4,5-dihydro-1H-1,2,3-triazole-4-carbaldehyde

: 1613039-83-0
N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

Guidance literature:: With sodium hydrogencarbonate; In ethanol; at 60 ℃;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 910546-48-4
(1-(4-methoxyphenyl)-1H-(1,2,3)triazol-4-yl)methanol

: 1613039-83-0
N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 0.58 h / 0 °C

2: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; sodium hydrogencarbonate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 2101-87-3
p-methoxy-phenylazide

: 1613039-83-0
N-((1-(4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methylene)-2-methylpropan-2-amine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: copper diacetate / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere

2: Jones reagent / acetone / 0.58 h / 0 °C

3: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; copper diacetate; sodium hydrogencarbonate; In ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2014.04.052