C₁₉H₃₄N₂O₄

Base Information

Chemical Name:C₁₉H₃₄N₂O₄
CAS No.:877758-78-6
Molecular Formula:C₁₉H₃₄N₂O₄
Molecular Weight:354.49
Hs Code.:

C<sub>19</sub>H<sub>34</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₉H₃₄N₂O₄

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Chemical Property of C₁₉H₃₄N₂O₄

Chemical Property:

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Technology Process of C₁₉H₃₄N₂O₄

There total 11 articles about C₁₉H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877665-38-8
ethyl trans-4-[1-tert-butoxycarbonyl-(5S)-(4-morpholinyl)methyl-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

: 877758-78-6
C₁₉H₃₄N₂O₄

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; for 3h;
DOI:10.1016/j.bmc.2012.11.003

Reference yield:

: 138528-06-0
(2S,5S)-5-benzyloxymethyl-1-tert-butoxycarbonyl-2-hydroxymethylpyrrolidine

: 877758-78-6
C₁₉H₃₄N₂O₄

Guidance literature:: Multi-step reaction with 12 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / 2 h / 60 °C

2: hydrogen; palladium(II) hydroxide / acetic acid; ethanol / 120 h / 20 °C / 1?atm

3: trifluoroacetic acid / dichloromethane / 0.67 h / 0 - 20 °C

4: Rh/Al₂O₃; trifluoroacetic acid; hydrogen / acetic acid; ethanol / 20 °C / 10?atm

5: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

6: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 °C

7: sodium hydride / N,N-dimethyl-formamide; ethanol / 0.67 h / 0 °C

8: potassium carbonate / water / 0.5 h / 70 °C

9: hydrogen; palladium(II) hydroxide / acetic acid; ethanol / 20 °C / 1?atm

10: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 - 20 °C

11: sodium tris(acetoxy)borohydride / tetrahydrofuran / 2.5 h / 20 °C

12: hydrogenchloride; water / 1,4-dioxane / 3 h

With hydrogenchloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; di-isopropyl azodicarboxylate; trichloroisocyanuric acid; Rh/Al₂O₃; water; hydrogen; palladium(II) hydroxide; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; 1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2012.11.003

Reference yield:

: 1416961-17-5
ethyl 4-[(5S)-benzyloxymethyl-1-tert-butoxycarbonyl-(2S)-pyrrolidinylmethoxy]benzoate

: 877758-78-6
C₁₉H₃₄N₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1: hydrogen; palladium(II) hydroxide / acetic acid; ethanol / 120 h / 20 °C / 1?atm

2: trifluoroacetic acid / dichloromethane / 0.67 h / 0 - 20 °C

3: Rh/Al₂O₃; trifluoroacetic acid; hydrogen / acetic acid; ethanol / 20 °C / 10?atm

4: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

5: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 °C

6: sodium hydride / N,N-dimethyl-formamide; ethanol / 0.67 h / 0 °C

7: potassium carbonate / water / 0.5 h / 70 °C

8: hydrogen; palladium(II) hydroxide / acetic acid; ethanol / 20 °C / 1?atm

9: trichloroisocyanuric acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 - 20 °C

10: sodium tris(acetoxy)borohydride / tetrahydrofuran / 2.5 h / 20 °C

11: hydrogenchloride; water / 1,4-dioxane / 3 h

With hydrogenchloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; Rh/Al₂O₃; water; hydrogen; palladium(II) hydroxide; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.11.003