(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

Base Information

Chemical Name:(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide
CAS No.:872175-11-6
Molecular Formula:C₂₃H₂₈N₄O₅
Molecular Weight:440.499
Hs Code.:

Synonyms:(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

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Technology Process of (4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

There total 4 articles about (4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872175-10-5
(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid dimethyl ester

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 872175-11-6
(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

Guidance literature:: With isopropylmagnesium bromide; In tetrahydrofuran; at -28 ℃; for 0.333333h;
DOI:10.1002/adsc.200404286

Reference yield:

: 872175-09-2
(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid

: 872175-11-6
(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / chlorotrimethylsilane / 12 h / 20 °C

2: iPrMgBr / tetrahydrofuran / 0.33 h / -28 °C

With chloro-trimethyl-silane; isopropylmagnesium bromide; In tetrahydrofuran;
DOI:10.1002/adsc.200404286

Reference yield:

: (4S,5R)-1,3-dibenzyl-5-(cyclohexyloxycarbonyl)-2-oxoimidazolidine-4-carboxylic acid

: 872175-11-6
(4S,5S)-1,3-dibenzylimidazolidin-2-one-4,5-dicarboxylic acid bis(methoxymethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / MeONa / methanol / 4 h / Heating

2: 95 percent / aq. NaOH / 1 h / Heating

3: 95 percent / chlorotrimethylsilane / 12 h / 20 °C

4: iPrMgBr / tetrahydrofuran / 0.33 h / -28 °C

With sodium hydroxide; chloro-trimethyl-silane; isopropylmagnesium bromide; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1002/adsc.200404286