2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

Base Information

Chemical Name:2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon
CAS No.:110372-68-4
Molecular Formula:C₃₆H₄₈O₅SSi
Molecular Weight:620.926
Hs Code.:

Synonyms:2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

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Chemical Property of 2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

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Technology Process of 2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

There total 3 articles about 2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110372-63-9
1D-(1,2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsiloxy)methyl>-5-C-(ethylthio)-1,2,3,4-cyclohexantetrol

: 110372-68-4
2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

Guidance literature:: With acetic anhydride; dimethyl sulfoxide; for 14h; Ambient temperature;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 110372-68-4
2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / dimethylformamide / 1.) 0 deg C, 30 min 2.) RT, 9 h

2: 90 percent / DMSO, Ac₂O / 14 h / Ambient temperature

With pyridine; acetic anhydride; dimethyl sulfoxide; In N,N-dimethyl-formamide;

Reference yield:

: 107960-18-9,110453-99-1
(2S,3R,4S,5S)-2,3,4-Tris-benzyloxy-5-ethylsulfanyl-5-hydroxymethyl-cyclohexanol

: 110372-68-4
2D-(2,4,5S/3,5C)-2,3,4-Tri-O-benzyl-5-C-<(tert-butyldimethylsilyloxy)methyl>-5-C-(ethylthio)-2,3,4-trihydroxy-1-cyclohexanon

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / dimethylformamide / 1.) 0 deg C, 30 min 2.) RT, 9 h

2: 90 percent / DMSO, Ac₂O / 14 h / Ambient temperature

With pyridine; acetic anhydride; dimethyl sulfoxide; In N,N-dimethyl-formamide;