ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

Base Information

Chemical Name:ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate
CAS No.:915030-29-4
Molecular Formula:C₁₅H₁₄F₃N₃O₃
Molecular Weight:341.29
Hs Code.:

Synonyms:ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

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Chemical Property of ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

Chemical Property:

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Technology Process of ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

There total 3 articles about ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 209991-63-9
2,4,6-trifluorophenylacetic acid

: 54147-04-5
5-amino-1-methyl-1H-imidazole-4-carboxylic acid ethyl ester

: 915030-29-4
ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

Guidance literature:: With 2,2-dimethylpropanoic anhydride; at 85 ℃; for 23h;

Reference yield:

: C₈H₁₆N₂O₃

: 915030-29-4
ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; acetonitrile / 18 h / 20 °C

2: 2,2-dimethylpropanoic anhydride / 23 h / 85 °C

With 2,2-dimethylpropanoic anhydride; In ethanol; acetonitrile;

Reference yield:

: 72809-03-1,150408-87-0
ethyl 2,3-diamino propionate

: 915030-29-4
ethyl 1-methyl-5-{[(2,4,6-trifluorophenyl)acetyl]amino}-1H-imidazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 1 - 1.17 h / 90 °C

2: ethanol; acetonitrile / 18 h / 20 °C

3: 2,2-dimethylpropanoic anhydride / 23 h / 85 °C

With 2,2-dimethylpropanoic anhydride; In ethanol; acetonitrile;