2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

Base Information

Chemical Name:2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide
CAS No.:1508310-56-2
Molecular Formula:C₂₀H₂₆N₂O₃S
Molecular Weight:374.504
Hs Code.:

Synonyms:2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

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Chemical Property of 2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

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Technology Process of 2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

There total 12 articles about 2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₄N₂O₃S

: 1508310-56-2
2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

Guidance literature:: With sodium tetrahydroborate; In methanol; Inert atmosphere;
DOI:10.1021/ml4003875

Reference yield:

: 107-10-8,42939-71-9
propylamine

: 1508310-55-1
2-[4-(ethylsulfonyl)phenyl]-N-(4-formylphenyl)acetamide

: 1508310-56-2
2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

Guidance literature:: propylamine; 2-[4-(ethylsulfonyl)phenyl]-N-(4-formylphenyl)acetamide; With sodium sulfate; In dichloromethane; at 20 ℃; Inert atmosphere;

With methanol; sodium tetrahydroborate; at 20 ℃; for 3h;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1508310-56-2
2-[4-(ethylsulfonyl)phenyl]-N-{4-[(propylamino)methyl]phenyl}acetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / toluene / 2 h / 143 °C / Dean-Stark

2.1: hydrogen / methanol; tetrahydrofuran / 4.5 h / 35 °C / 30003 Torr

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C

3.2: 2 h / 20 °C

4.1: sodium sulfate / dichloromethane / 72 h / 20 °C

5.1: sodium tetrahydroborate / methanol / Inert atmosphere

With sodium tetrahydroborate; hydrogen; benzotriazol-1-ol; toluene-4-sulfonic acid; sodium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ml4003875