methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

Base Information

Chemical Name:methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate
CAS No.:160462-37-3
Molecular Formula:C₂₂H₂₆BrClO₃
Molecular Weight:453.804
Hs Code.:

Synonyms:methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

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Chemical Property of methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

Chemical Property:

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Technology Process of methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

There total 14 articles about methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53088-68-9
methyl 3-chlorophenylacetate

: 160462-37-3
methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

Guidance literature:: Multi-step reaction with 3 steps

1: NBS, AIBN / CCl₄ / Heating

2: Cs₂CO₃ / dimethylformamide

3: Ph₃P, CBr₄ / CH₂Cl₂

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); carbon tetrabromide; caesium carbonate; triphenylphosphine; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00075a033

Reference yield:

: 53596-60-4
methyl 3-allyl-4-hydroxybenzoate

: 160462-37-3
methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / K₂CO₃ / acetone / Heating

2: 94 percent / 2,6-di-tert-butyl-4-methylphenol (BHT) / various solvent(s) / Heating

3: 97 percent / Et₃N, DMAP / CH₂Cl₂

4: 90 percent / H₂ / 5percent Rh/C / ethanol

5: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

6: 88 percent / n-Bu₄NF / tetrahydrofuran

7: Cs₂CO₃ / dimethylformamide

8: Ph₃P, CBr₄ / CH₂Cl₂

With dmap; lithium aluminium tetrahydride; carbon tetrabromide; 2,6-di-tert-butyl-4-methyl-phenol; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; caesium carbonate; triethylamine; triphenylphosphine; Rh on carbon; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00075a033

Reference yield:

: 35750-24-4
methyl 4-allyloxybenzoate

: 160462-37-3
methyl 2-(2,6-Dipropyl-4-Bromomethylphenoxy)-2-(3-Chlorophenyl)Acetate

Guidance literature:: Multi-step reaction with 9 steps

1: 90 percent / 2,6-di-tert-butyl-4-methylphenol (BHT) / various solvent(s) / Heating

2: 87 percent / K₂CO₃ / acetone / Heating

3: 94 percent / 2,6-di-tert-butyl-4-methylphenol (BHT) / various solvent(s) / Heating

4: 97 percent / Et₃N, DMAP / CH₂Cl₂

5: 90 percent / H₂ / 5percent Rh/C / ethanol

6: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

7: 88 percent / n-Bu₄NF / tetrahydrofuran

8: Cs₂CO₃ / dimethylformamide

9: Ph₃P, CBr₄ / CH₂Cl₂

With dmap; lithium aluminium tetrahydride; carbon tetrabromide; 2,6-di-tert-butyl-4-methyl-phenol; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; caesium carbonate; triethylamine; triphenylphosphine; Rh on carbon; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00075a033