2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

Base Information

Chemical Name:2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol
CAS No.:1407968-91-5
Molecular Formula:C₃₇H₄₆O₂Si
Molecular Weight:550.857
Hs Code.:

Synonyms:2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

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Chemical Property of 2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

Chemical Property:

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Technology Process of 2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

There total 1 articles about 2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 799-13-3
bis(5-tert-butyl-2-hydroxyphenyl)methane

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1407968-91-5
2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1407968-91-5
2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

: 1407968-92-6
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

Guidance literature:: 2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol; With triethylamine; magnesium chloride; In acetonitrile; at 20 ℃; for 0.25h;

formaldehyd; In acetonitrile; for 24h; Reflux;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407968-91-5
2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

: 1407968-93-7
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

1.2: 24 h / Reflux

2.1: potassium carbonate / acetonitrile / 24 h / Reflux

With potassium carbonate; triethylamine; magnesium chloride; In acetonitrile;
DOI:10.1016/j.tet.2012.09.032