3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

Base Information

Chemical Name:3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde
CAS No.:1407968-93-7
Molecular Formula:C₄₅H₅₂O₃Si
Molecular Weight:668.992
Hs Code.:

Synonyms:3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

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Chemical Property of 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

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Technology Process of 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

There total 4 articles about 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1407968-92-6
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

: 100-39-0
benzyl bromide

: 1407968-93-7
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

Guidance literature:: With potassium carbonate; In acetonitrile; for 24h; Reflux;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 799-13-3
bis(5-tert-butyl-2-hydroxyphenyl)methane

: 1407968-93-7
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

2.2: 24 h / Reflux

3.1: potassium carbonate / acetonitrile / 24 h / Reflux

With 1H-imidazole; potassium carbonate; triethylamine; magnesium chloride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407968-91-5
2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

: 1407968-93-7
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-2-(benzyloxy)-5-tertbutylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

1.2: 24 h / Reflux

2.1: potassium carbonate / acetonitrile / 24 h / Reflux

With potassium carbonate; triethylamine; magnesium chloride; In acetonitrile;
DOI:10.1016/j.tet.2012.09.032