3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

Base Information

Chemical Name:3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde
CAS No.:1407968-92-6
Molecular Formula:C₃₈H₄₆O₃Si
Molecular Weight:578.867
Hs Code.:

Synonyms:3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

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Chemical Property of 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

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Technology Process of 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

There total 3 articles about 3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1407968-91-5
2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

: 1407968-92-6
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

Guidance literature:: 2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol; With triethylamine; magnesium chloride; In acetonitrile; at 20 ℃; for 0.25h;

formaldehyd; In acetonitrile; for 24h; Reflux;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 799-13-3
bis(5-tert-butyl-2-hydroxyphenyl)methane

: 1407968-92-6
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

2.2: 24 h / Reflux

With 1H-imidazole; triethylamine; magnesium chloride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1407968-92-6
3-(5-tert-butyl-2(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2.1: magnesium chloride; triethylamine / acetonitrile / 0.25 h / 20 °C

2.2: 24 h / Reflux

With 1H-imidazole; triethylamine; magnesium chloride; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.09.032