2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Base Information

Chemical Name:2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?
CAS No.:1428847-54-4
Molecular Formula:C₁₆H₂₁NO₉S
Molecular Weight:403.41
Hs Code.:

Synonyms:2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Suppliers and Price of 2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

There total 6 articles about 2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid? which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428847-53-3
2-(benzyloxy)-2-oxoethyl 3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoate

: 1428847-54-4
2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; for 3h; under 1034.32 Torr;

Reference yield:

: 24812-90-6
methyl 3-amino-4-methoxybenzoate

: 1428847-54-4
2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 2 h / 20 °C

2: dmap / dichloromethane / 2 h / 20 °C

3: tin(II) chloride dihdyrate; lithium hydroxide / tetrahydrofuran / 24 h / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C

5: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 3 h / 1034.32 Torr

With pyridine; dmap; tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;

Reference yield:

: 29655-68-3
methyl 4-methoxy-3-(methylsulfonamido)benzoate

: 1428847-54-4
2-(3-(N-(tert-butoxycarbonyl)methylsulfonamido)-4-methoxybenzoyloxy)acetic acid?

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / dichloromethane / 2 h / 20 °C

2: tin(II) chloride dihdyrate; lithium hydroxide / tetrahydrofuran / 24 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 3 h / 1034.32 Torr

With dmap; tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;